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AbstractAbstract
[en] The experimental research work was carried out in accordance with the Factorial Design Statistical Method to evaluate and analyze the influence of calcium, magnesium, silica and phosphorus on the precipitation of vanadates. precipitation was performed by neutralization with H2 SO4 of alkaline aqueous solutions containing vanadium pentoxide (V2 O5) at 60 ± 2 deg C. The experimental responses measured were percent of vanadium recovery and vanadium pentoxide content in the precipitate. These impurities are considered representative of those present in a leach liquor from the ore obtained at Campo Alegre de Lourdes (Brazil). The operational variables in this work were used optimum conditions as determined by the statistical approach. Among the impurities under study, phosphorus exhibited the highest negative influence on the experimental responses. Phosphorus diminished the percent of vanadium recovered from 98.9 to 34.5 and the vanadium oxide content in the precipitate from 91.2% to 39.3%. (author)
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Source
13 refs., 8 tabs. Electronic journal available in www.scielo.br
Record Type
Journal Article
Journal
Brazilian Journal of Chemical Engineering; ISSN 0104-6632; ; v. 17(2); [13 p.]
Country of publication
ALKALINE EARTH METALS, CHALCOGENIDES, CHEMICAL ANALYSIS, COHERENT SCATTERING, DIFFRACTION, ELEMENTS, EXTRACTIVE METALLURGY, HYDROGEN COMPOUNDS, INORGANIC ACIDS, INORGANIC COMPOUNDS, METALLURGY, METALS, MINERALS, NONMETALS, OXIDE MINERALS, OXIDES, OXYGEN COMPOUNDS, QUANTITATIVE CHEMICAL ANALYSIS, SCATTERING, SILICON COMPOUNDS, SILICON OXIDES, SULFUR COMPOUNDS, TRANSITION ELEMENT COMPOUNDS, TRANSITION ELEMENTS, VANADIUM COMPOUNDS, VOLUMETRIC ANALYSIS
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