[en] Hydridable metal alloys are used at the Savannah River Site to process tritium. The goal of this work was to develop a mechanical alloying process as a low-cost option to produce these alloys on-site. High-speed milling at elevated temperatures has the potential to significantly reduce the time and cost of the mechanical alloying process. It was demonstrated that elemental metal powders can be alloyed in an attritor mill under argon. In order to form LaNi_4.25Al_0.75 from elemental metals it was found that lanthanum and nickel must be alloyed prior to adding aluminum. It was also demonstrated that metal powders could be alloyed in the high-speed attritor with the temperature in the mill equilibrating at ∼220 C. Optimization of the process parameters will require additional testing