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Zainab Ramli; Sheela Chandren
The Malaysian Analytical Sciences Society (ANALIS), International Education Center (INTEC), UiTM Shah Alam, Selangor (Malaysia)2007
The Malaysian Analytical Sciences Society (ANALIS), International Education Center (INTEC), UiTM Shah Alam, Selangor (Malaysia)2007
AbstractAbstract
[en] Organized meso porous materials represent a class of molecular sieves because of its high potential for commercial applications in adsorption and catalysis. In this study, organized meso porous alumina was synthesized by the sol-gel method using various organic templates, i.e. cationic, neutral and anionic surfactants. Surface porosity of the synthesized alumina obtained exhibit materials in the meso pore ranges. The morphology of the samples consists of wormhole-like meso structure in the nano-region (20 - 70 nm). Sample with cetyl trimethylammonium bromide as cationic templates has the narrowest pore distribution centred at 8 nm as compared to samples synthesized with Triton X-114 (neutral) and stearic acid (anionic). All samples showed only Lewis acidity. Acidity and meso porous character present in these meso porous alumina samples showed that this material has potential as catalyst support and also used in Lewis acid catalyzed reactions. Study showed that the cationic surfactant is a better template to obtain uniform meso porous alumina that might be due to the weak interaction between the template and the surface of the alumina. (author)
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5 figs. 1 tab. Abstract and full text available in http://pkukmweb.ukm.my/mjas/; Official journal of The Malaysian Analytical Sciences Society (ANALIS)
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Journal Article
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Malaysian Journal of Analytical Sciences; ISSN 1394-2506; ; v. 11(1); p. 110-116
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