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Gomay, Yoshio; Tazima, Teruhiko; Satake, Toru; Mizuno, Masayasu.
Japan Atomic Energy Research Inst., Tokyo1977
Japan Atomic Energy Research Inst., Tokyo1977
AbstractAbstract
[en] For tokamak wall conditioning, surface cleaning of molybdenum by chemical reaction with oxygen and hydrogen gases has been studied experimentally by Auger electron spectroscopy (AES) and Auger/Sputter techniques. Means of pretreatments, buffering with water containing Al2O3 powder, glow discharge cleaning, and electropolishing show similar results. By exposing molybdenum sample to 0.1 Torr oxygen and 1 Torr hydrogen successively at 5000C, the impurity content on the surface reduces to 1/3 -- 1/4 of the initial value. When the content is reduced below the detectable limit of AES by heating up to 1,8000C in vacuum, it becomes 1/6 -- 1/7. By heating at 5000C, the impurities in the surface penetrate inward, probably because of the increase of impurity diffusion at this temperature. (auth.)
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Nov 1977; 17 p
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