[en] The synthesis of no-carrier-added 3-[¹⁸F]fluoroanisole, 2-[¹⁸F]fluoroanisole, [¹⁸F]fluorobenzene and 4-[¹⁸F]fluoroveratrole are reported. The strategy consists of amino-polyether supported nucleophilic substitution with [¹⁸F]F^- on activated nitro aromatic aldehyde precursors followed by decarbonylation using Tris(triphenylphosphine) rhodium (I) chloride. The experimental parameters for this reaction have been studied and optimized with 2-[¹⁸F]fluoro-4-methoxybenzaldehyde and then successfully applied to four other ¹⁸F-fluorinated aromatic aldehydes. The decarbonylation yields obtained were 84±5% (corrected for decay) within 15 min at 150^oC in 1,4-dioxan. (author)